"Influence of Alloy Composition on the Process Robustness of Steels Con" by Jonathan Kelley
 

Masters Theses

Keywords and Phrases

Alloy design; High-strength low-alloy steel; Laser-directed energy deposition; Powder blend; Robustness; Sensitivity analysis

Abstract

"To ensure consistent quality of additively manufactured parts, it is advantageous to identify alloys which can meet performance criteria while being robust to process variations. Toward this end, this work investigated the effect of alloy composition on the robustness of steels consolidated via laser-directed energy deposition (L-DED). Ultra-high-strength low-alloy steel (UHSLA) and pure iron powders were mixed in-situ to produce 10 compositions containing 10-100% UHSLA by mass. JMatPro material simulations roughly predicted phases and mechanical properties. Two sets of experiments were used to evaluate the sensitivity of as-built hardness (all 10 compositions) and tensile properties (5 select compositions) to process parameters. The hardness sensitivity peaked at 40-50% UHSLA, corresponding to phase fluctuations between lath martensite and upper bainite depending on the cooling rate. Lower (≤20%) or higher (≥70%) alloy contents were generally less sensitive, transforming primarily to ferrite or martensite, respectively, with auto-tempering of martensite at lower cooling rates. The ultimate tensile strength (UTS) and yield strength (YS) sensitivities followed a similar trend up to 70% UHSLA, beyond which the YS sensitivity remained low while the UTS sensitivity increased, corresponding to variations in the work hardening behavior. This may reveal that the work hardening capability at higher alloy contents is particularly sensitive to factors such as auto-tempering and/or grain size. A robust compositional balance (70%) avoided martensite/bainite fluctuations while minimizing other microstructural sensitivities. The 70% mixture also represented a minimum alloy content at which ductility could be improved without sacrificing tensile toughness. While its high strength (UTS 1,296 MPa) was lower than that of UHSLA (UTS 1,632 MPa), its improved elongation (21.7%) over UHSLA (16.9%) caused its tensile toughness to about match that of UHSLA. This work demonstrates the efficacy of a methodology for incorporating robust design into the rapid evaluation of alloys for metal additive manufacturing"--Abstract, p. iii

Advisor(s)

Liou, Frank W.

Committee Member(s)

Newkirk, Joseph William
Leu, M. C. (Ming-Chuan)

Department(s)

Mechanical and Aerospace Engineering

Degree Name

M.S. in Manufacturing Engineering

Publisher

Missouri University of Science and Technology

Publication Date

Spring 2025

Pagination

xii, 127 pages

Note about bibliography

Includes_bibliographical_references_(pages 120-126)

Rights

©2023 Jonathan Kelley , All Rights Reserved

Document Type

Thesis - Open Access

File Type

text

Language

English

Thesis Number

T 12485

Included in

Manufacturing Commons

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