Abstract
Phenol–formaldehyde (phenolic) thermosets are known for excellent heat and chemical resistance, high flame retardance, and good mechanical performance. However, phenolics are also known for their high brittleness, and tendency to form voids, due to a condensation reaction forming water during curing. These voids can decrease the mechanical performance of the resultant phenolic composite and introduce undesirable performance characteristics. This work aims to develop a technique that uses high-pressure infiltration to obtain dense phenolic matrix composites, with commercially available resin and fiber reinforcement. The high-pressure system developed in this work is compared to a conventional low-pressure resin infusion technique, and the porosity after each infusion is analyzed. A model of the low- and high-pressure systems was developed, and the predicted time of infiltration was compared to the experimental results. The high-pressure system had 97% less open porosity after infusion than the low-pressure technique, suggesting that it can produce a higher-quality and better-performing phenolic composite than conventional techniques. Also, the mechanical test performed indicates improved performance for the high-pressure injection with a 30.73% increase in ultimate tensile strength in comparison to low pressure, indicating better mechanical performance. © 2024 Society of Industrial Chemistry.
Recommended Citation
S. Weiler et al., "Development Of A High-Pressure Infiltration Process For Phenol–formaldehyde Matrix Composites," Polymer International, Wiley; Society of Chemical Industry, Jan 2024.
The definitive version is available at https://doi.org/10.1002/pi.6623
Department(s)
Mechanical and Aerospace Engineering
Publication Status
Full Access
Keywords and Phrases
composite; high pressure; infusion; low pressure; phenolics
International Standard Serial Number (ISSN)
1097-0126; 0959-8103
Document Type
Article - Journal
Document Version
Citation
File Type
text
Language(s)
English
Rights
© 2024 Wiley; Society of Chemical Industry, All rights reserved.
Publication Date
01 Jan 2024