Abstract
Nanostructured Steels Are Expected to Have Enhanced Irradiation Tolerance and Improved Strength. However, They Suffer from Poor Microstructural Stability at Elevated Temperatures. in This Study, Fe–21Cr–5Al–0.026C (Wt%) Kanthal D (KD) Alloy Belonging to a Class of (FeCrAl) Alloys Considered for Accident-Tolerant Fuel Cladding in Light-Water Reactors is Nanostructured using Two Severe Plastic Deformation Techniques of Equal-Channel Angular Pressing (ECAP) and High-Pressure Torsion (HPT), and their Thermal Stability between 500–700 °C is Studied and Compared. ECAP KD is Found to Be Thermally Stable Up to 500 °C, Whereas HPT KD is Unstable at 500 °C. Microstructural Characterization Reveals that ECAP KD Undergoes Recovery at 550 °C and Recrystallization above 600 °C, While HPT KD Shows Continuous Grain Growth after Annealing above 500 °C. Enhanced Thermal Stability of ECAP KD is from Significant Fraction (>50%) of Low-Angle Grain Boundaries (GBs) (Misorientation Angle 2–15°) Stabilizing the Microstructure Due to their Low Mobility. Small Grain Sizes, a High Fraction (>80%) of High-Angle GBs (Misorientation Angle >15°) and Accordingly a Large Amount of Stored GB Energy, serve as the Driving Force for HPT KD to Undergo Grain Growth Instead of Recrystallization Driven by Excess Stored Strain Energy.
Recommended Citation
M. Arivu et al., "Comparison of the Thermal Stability in Equal-Channel-Angular-Pressed and High-Pressure-Torsion-Processed Fe–21Cr–5Al Alloy," Advanced Engineering Materials, Wiley; Wiley-VCH Verlag, Jan 2023.
The definitive version is available at https://doi.org/10.1002/adem.202300756
Department(s)
Mechanical and Aerospace Engineering
Second Department
Materials Science and Engineering
Publication Status
Full Access
Keywords and Phrases
grain growth; microstructural characterization; microstructural characterization; nanostructured steels; sever plastic deformation recrystallization
International Standard Serial Number (ISSN)
1527-2648; 1438-1656
Document Type
Article - Journal
Document Version
Citation
File Type
text
Language(s)
English
Rights
© 2023 Wiley; Wiley-VCH Verlag, All rights reserved.
Publication Date
01 Jan 2023
Included in
Aerospace Engineering Commons, Materials Science and Engineering Commons, Mechanical Engineering Commons
Comments
U.S. Department of Energy, Grant NRC 31310018M0044