Plasma Spheroidization of Vitreloy 106A Bulk Metallic Glass Powder
Abstract
Inert ground Vitreloy 106A powder was used as the starting material for inductively coupled plasma spheroidization. The processed powders were characterized to determine their morphology, flowability, chemistry, and thermal transitions. Processed powder samples were shown to have a particle size distribution that was consistent with the starting material indicating that no significant agglomeration of particles occurred. The average circularity of the processed powder increased when compared to the starting powder. This resulted in higher apparent and tap densities and the flowability also increased. Fine particles that were high in oxygen and copper were vaporized resulting in tightening of the chemistry distribution. XRD and DSC indicated that the starting powder was fully crystallized while the processed powder had both amorphous and crystalline structures present. Raman spectroscopy was used to detect NiO on the surface of the processed powder particles. Powder characterization indicated that the processed powder had better properties compared to the starting powder when considering flowability, amorphous content, and sphericity.
Recommended Citation
C. S. Kriewall and J. W. Newkirk, "Plasma Spheroidization of Vitreloy 106A Bulk Metallic Glass Powder," Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science, vol. 50, no. 10, pp. 4791 - 4797, Springer Boston, Oct 2019.
The definitive version is available at https://doi.org/10.1007/s11661-019-05405-8
Department(s)
Materials Science and Engineering
Keywords and Phrases
Compressive Strength; Inductively Coupled Plasma; Morphology; Nickel Oxide; Particle Size; Particle Size Analysis, Amorphous Content; Bulk Metallic Glass; Crystalline Structure; Plasma Spheroidization; Powder Characterization; Powder Particles; Starting Powders; Thermal Transitions, Metallic Glass
International Standard Serial Number (ISSN)
1073-5623; 1543-1940
Document Type
Article - Journal
Document Version
Citation
File Type
text
Language(s)
English
Rights
© 2019 The Minerals, Metals & Materials Society and ASM International, All rights reserved.
Publication Date
01 Oct 2019
Comments
This work was funded by Honeywell Federal Manufacturing & Technologies under Contract No. DE-NA0002839 with the U.S. Department of Energy.