Masters Theses
Keywords and Phrases
Additive Manufacturing; Boron Carbide; Freeze-form Extrusion Fabrication
Abstract
"Boron carbide is a safe, alternative to beryllium as a material for aerospace structures since it is also light-weight and exhibits high strength. This paper discusses a study of the Freeze-form Extrusion Fabrication (FEF) process to fabricate parts from boron carbide. Process parameters and hardware were modified to fabricate boron carbide specimens free of printed defects. Four-point bending tests were performed to measure the flexural strength of fabricated specimens. Observations of the presence of voids caused by ice crystals in fabricated parts led to further development and characterization of the boron carbide paste used with the FEF process. Additives were selected and tested to observe their effect on the size of the ice-crystal voids. Scanning electron microscopy was used to observe the voids left from the ice crystals after part sintering. Post-image analysis was performed to measure approximate sizes of ice-crystal voids and these results were summed up in a void size distribution. Glycerol in a concentration of 25 wt% by water increased the flexural strength of test bars from 58.1 MPa to 67.4 MPa and the sintered relative density from 76.2% to 85.0%. The standard deviation of the flexural strength decreased from 23.0 to 14.5 MPa. None of the additives considered reduced the sizes of the ice crystal voids desirably as the highest relative density of the sintered test bars achieved was only 85.0%."--Abstract, page iii.
Advisor(s)
Leu, M. C. (Ming-Chuan)
Landers, Robert G.
Committee Member(s)
Hilmas, Greg
Department(s)
Mechanical and Aerospace Engineering
Degree Name
M.S. in Mechanical Engineering
Publisher
Missouri University of Science and Technology
Publication Date
Summer 2015
Pagination
ix, 81 pages
Note about bibliography
Includes bibliographical references (pages 78-80).
Rights
© 2015 Aaron Scott Thornton, All rights reserved.
Document Type
Thesis - Open Access
File Type
text
Language
English
Subject Headings
Ceramic materials -- ExtrusionSolid freeform fabricationManufacturing processes
Thesis Number
T 10744
Electronic OCLC #
921186546
Recommended Citation
Thornton, Aaron Scott, "Freeze-form extrusion fabrication of boron carbide" (2015). Masters Theses. 7439.
https://scholarsmine.mst.edu/masters_theses/7439