Masters Theses
Abstract
"The effect of lead oxide additions on sintering characteristics and dielectric properties of ferroelectric Pb3MgNb2O9 based capacitors was studied. The basic dielectric compositions were formed by solid state reaction. Densification was studied as a function of PbO content over the temperature range 900 °C to 1000 °C for sintering times one to six hours depending on the amount of additive, and the sintering temperature.
Weight loss, density and shrinkage measurements of each composition were made in order to relate the effects of the excess PbO additions on the densification. The dielectric and electrical properties were then correlated to the micro structure and density.
The compositions sintered at low temperatures were densified by the formation of a liquid phase during sintering. However, an increase of the amount of liquid phase does not necessarily yield optimum dielectric properties. A proper control of the sintering temperature, time and the amount of excess PbO is required for optimization of the dielectric properties"--Abstract, page ii.
Advisor(s)
Anderson, H. U. (Harlan U.)
Committee Member(s)
Guha, Jyoti, P.
Sparlin, Don M.
Department(s)
Materials Science and Engineering
Degree Name
M.S. in Ceramic Engineering
Publisher
University of Missouri--Rolla
Publication Date
Spring 1987
Pagination
ix, 62 pages
Note about bibliography
Includes bibliographical references (pages 49-54).
Rights
© 1987 Dyllan Jye-Lun Hong, All rights reserved.
Document Type
Thesis - Open Access
File Type
text
Language
English
Thesis Number
T 5474
Print OCLC #
16812428
Recommended Citation
Hong, Dyllan Jye-Lun, "The effect of excess lead oxide on the sintering characteristics and dielectric properties of lead magnesium niobate ceramics" (1987). Masters Theses. 460.
https://scholarsmine.mst.edu/masters_theses/460