"Effect Of Thermomechanical Processing And Heat Treatment On The Micros" by Rogerio Antao Cardoso
 

Doctoral Dissertations

Keywords and Phrases

Fe-Mn-Al; Martensite; NiAl; Strain accumulation; Tempered Martensite Embrittlement; Tempering

Abstract

"A martensite-based and an austenite-based Fe-Mn-Al steels were investigated aiming the pilot-scale production of steels that meet military specifications for Rolled Homogeneous Armor (RHA) and High-hardness Armor (HHA) plates. Each material underwent specific thermomechanical processes and the following hardness, Charpy V-notch (CVN) impact toughness at -40 °C and room-temperature tensile properties were correlated with the resulting microstructures.

Specimens of the martensitic steel were austenitized at 1010 °C, quenched and tempered at 150, 175, 200, 225 and 250 °C for times up to four hours. As for the Fe-Mn-Al steel, its hot rolling schedule was design to promote strain accumulation in the as-rolled matrix, which is conducive to the precipitation of NiAl during annealing heat treatments. Specimens of this steel were annealed at 700, 750, 800 and 900 °C for times up to one hour.

The results show evidence of tempered martensite embrittlement (TME) in the martensite-based steel, especially when tempered for four hours at the investigated temperature range.

Regarding the Fe-Mn-Al steel, electron backscattered analyses (EBSD) revealed strain accumulation in the as-rolled austenitic matrix. Annealing at 750 °C for 30 min. strengthened the steel through intra-granular precipitation of NiAl. It was followed by a drop in the CVN impact toughness. Nevertheless, literature review showed that the investigated material outperformed similar austenite-based Fe-Mn-Al steels strengthened through k-carbide"--Abstract, p. iv

Advisor(s)

Bartlett, Laura

Committee Member(s)

Chandrashekhara, K.
Buchely, Mario F.
O'Malley, Ronald J.
Gu, Yijia

Department(s)

Materials Science and Engineering

Degree Name

Ph. D. in Materials Science and Engineering

Publisher

Missouri University of Science and Technology

Publication Date

Spring 2025

Pagination

xv, 131 pages

Note about bibliography

Includes_bibliographical_references_(pages 41, 74, 119 and 125-130)

Rights

©2024 Rogerio Antao Cardoso , All Rights Reserved

Document Type

Dissertation - Open Access

File Type

text

Language

English

Thesis Number

T 12454

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