Abstract

The high-resolution rotational spectrum of difluoro diiodomethane is reported for the first time. A molecular-beam broadband Fourier transform microwave spectrometer recorded the spectrum over the frequency range of 5.9–18.1 GHz. The rotational constants, centrifugal distortion constants, nuclear quadrupole coupling constants, and nuclear spin-rotation constants for the two equivalent iodine nuclei were determined from fitting 1378 hyperfine transitions of 163 rotational transitions: A = 2743.79691(18)MHz, B = 587.83103(5) MHz, C = 528.72470(5) MHz, χaa = −1213.287(6) MHz, χbb – χcc = −885.210(5) MHz, and χab = 1437.721(5) MHz. 31 dipole-forbidden/quadrupole-allowed transitions, arising from the large nuclear quadrupole coupling effect of iodine, were observed in the spectrum and assigned. Ab initio and quantum chemical calculations, at the MP2/aug-cc-pVTZ-pp and MP2//B3LYP/6-311G** levels of theory, were used to predict the rotational constants, centrifugal distortion constants, nuclear quadrupole coupling constants, and nuclear spin-rotation constants and guide the data analysis.

Department(s)

Chemistry

Publication Status

Open Access

Keywords and Phrases

Ab initio calculations; Difluorodiiodomethane; FTMW; Iodine nuclear quadrupole coupling constants; Microwave spectroscopy

International Standard Serial Number (ISSN)

1096-083X; 0022-2852

Document Type

Article - Journal

Document Version

Citation

File Type

text

Language(s)

English

Rights

© 2026 Elsevier, All rights reserved.

Publication Date

01 Oct 2026

Included in

Chemistry Commons

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