High-Pressure NMR Probes for the in situ Investigation of Gas/Liquid Reactions

Author

Klaus Woelk, Missouri University of Science and TechnologyFollow
Joachim Bargon

Abstract

Three different types of nuclear magnetic resonance (NMR) probes have been developed for investigating multiple phase (gas/liquid) reactions in situ at ambient and high pressure. Versions requiring only minimal modifications of existing NMR probes, low volume probes, and high precision flow systems have been optimized for specific boundary conditions. Pressures ranging from 1 to 20 bar have been successfully applied. The arrangements are especially attractive for the in situ investigations of homogeneous hydrogenation reactions displaying nuclear spin polarization.

Recommended Citation

K. Woelk and J. Bargon, "High-Pressure NMR Probes for the in situ Investigation of Gas/Liquid Reactions," Review of Scientific Instruments, vol. 63, no. 6, pp. 3307 - 3310, American Institute of Physics (AIP), Feb 1992.

The definitive version is available at https://doi.org/10.1063/1.1142543

Department(s)

Chemistry

International Standard Serial Number (ISSN)

0034-6748

Document Type

Article - Journal

Document Version

Citation

File Type

text

Language(s)

English

Rights

© 1992 American Institute of Physics (AIP), All rights reserved.

Publication Date

01 Feb 1992