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Title: Effect of operating conditions on the size, morphology, and concentration of submicrometer particulates emitted from a diesel engine
Author (s): Neer, Anthony Ronalk
Koylu, Umit
Department/Lab Affiliations: Mechanical & Aerospace Engineering
Space Systems Engineering
Keywords: Diesel engines
Emissions
Fractal morphology
Particle size
Particulate matter
Issue Date: 2006
Publisher: Elsevier / The Combustion Institute
Citation: Neer, A., and Koylu, U.O., “Effect of Operating Conditions on the Size, Morphology, and Concentration of Submicrometer Particulates Emitted from a Diesel Engine," Combustion and Flame 146: 142-154 (2006).
Abstract: Particulate emissions at the exhaust of a diesel engine were systematically investigated at different engine loads and speeds by rapid thermophoretic sampling followed by direct transmission electron microscope (TEM) visualization. Spherule and aggregate size distributions, aggregate fractal dimensions and prefactors, and particle volume fractions were comprehensively characterized using this novel technique, which provided new, accurate, and relevant data on diesel particulates compared to the abundant past studies involving questionable mobility sizing measurements. In contrast to the narrow (Gaussian) distributions of spherule sizes, there were broad variations in aggregate sizes that were approximated by a lognormal probability function with a geometric standard deviation of about 1.8. Mean spherule diameters were in the range 20–35 nm, and mean aggregate gyration diameters of 0.16–0.35 μm were always smaller than the PM2.5 standard. Average sizes of both spherules and aggregates mostly increased with the relative engine load or overall equivalence ratio, which disagreed with the trends and correlations suggested by a recent study. Independent of engine operating condition, aggregate fractal dimension was 1.77±0.14, a nearly universal property that contradicted with the broad range of past values reported for diesel engines based on mobility-based experiments. The aggregate fractal prefactor, which was also necessary to fully characterize the morphology of diesel soot, was found to be 1.9±0.5. In addition to this new contribution, sampling/TEM experiments were also implemented for the first time in a diesel engine to estimate particle volume fractions, which were crucial for the determination of available specific surface areas. The present method was more accurate than the laser attenuation method for the relatively low particle volume fractions of 0.001–0.1 ppm emitted by the diesel engine considered here.
Type: Article - Journal
text
In Title: Combustion and Flame
Copyright Notice: This material is presented to ensure timely dissemination of scholarly and technical work. Copyright and all rights therein are retained by authors or by other copyright holders. All persons copying this information are expected to adhere to the terms and constraints invoked by each author's copyright. In most cases, these works may not be reposted without the explicit permission of the copyright holder.
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http://www.elsevier.com/wps/find/journaldescription.cws_home/505736/authorinstructions
Publisher URL:
http://dx.doi.org/10.1016/j.combustflame.2006.04.003
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titleEffect of operating conditions on the size, morphology, and concentration of submicrometer particulates emitted from a diesel engine
contributor.authorNeer, Anthony Ronalk
contributor.authorKoylu, Umit
contributor.deptlabMechanical & Aerospace Engineering
contributor.deptlabSpace Systems Engineering
contributor.sponsorUniversity of Missouri Research Board
subjectDiesel engines
subjectEmissions
subjectFractal morphology
subjectParticle size
subjectParticulate matter
date.issued2006
publisherElsevier / The Combustion Institute
identifier.citationNeer, A., and Koylu, U.O., “Effect of Operating Conditions on the Size, Morphology, and Concentration of Submicrometer Particulates Emitted from a Diesel Engine," Combustion and Flame 146: 142-154 (2006).
identifier.pub.URI
http://dx.doi.org/10.1016/j.combustflame.2006.04.003
description.abstractParticulate emissions at the exhaust of a diesel engine were systematically investigated at different engine loads and speeds by rapid thermophoretic sampling followed by direct transmission electron microscope (TEM) visualization. Spherule and aggregate size distributions, aggregate fractal dimensions and prefactors, and particle volume fractions were comprehensively characterized using this novel technique, which provided new, accurate, and relevant data on diesel particulates compared to the abundant past studies involving questionable mobility sizing measurements. In contrast to the narrow (Gaussian) distributions of spherule sizes, there were broad variations in aggregate sizes that were approximated by a lognormal probability function with a geometric standard deviation of about 1.8. Mean spherule diameters were in the range 20–35 nm, and mean aggregate gyration diameters of 0.16–0.35 μm were always smaller than the PM2.5 standard. Average sizes of both spherules and aggregates mostly increased with the relative engine load or overall equivalence ratio, which disagreed with the trends and correlations suggested by a recent study. Independent of engine operating condition, aggregate fractal dimension was 1.77±0.14, a nearly universal property that contradicted with the broad range of past values reported for diesel engines based on mobility-based experiments. The aggregate fractal prefactor, which was also necessary to fully characterize the morphology of diesel soot, was found to be 1.9±0.5. In addition to this new contribution, sampling/TEM experiments were also implemented for the first time in a diesel engine to estimate particle volume fractions, which were crucial for the determination of available specific surface areas. The present method was more accurate than the laser attenuation method for the relatively low particle volume fractions of 0.001–0.1 ppm emitted by the diesel engine considered here.
typeArticle - Journal
type.DCMITypetext
type.statusPostprint
rightsThis material is presented to ensure timely dissemination of scholarly and technical work. Copyright and all rights therein are retained by authors or by other copyright holders. All persons copying this information are expected to adhere to the terms and constraints invoked by each author's copyright. In most cases, these works may not be reposted without the explicit permission of the copyright holder.
rights.URI
http://www.elsevier.com/wps/find/journaldescription.cws_home/505736/authorinstructions
relation.isPartOfCombustion and Flame
date.accessioned2007-04-11T17:00:48Z
date.available2008-05-12T21:38:41Z
identifier.persist.URI
http://scholarsmine.mst.edu/post_prints/EffectofOperatingConditionsontheSizeMorphology_09007dcc804f2af3.html