Microstructure of Thin Iron Carbide Films Prepared in a Glow Discharge
Thin (50-80 nm) iron carbide films were grown on carbon-coated copper grids in an r.f. glow discharge using iron pentacarbonyl and hydrogen as starting materials. The substrate temperatures were varied in the range 200-500 °C. The microstructure and phases present in these films are compared with the corresponding results previously obtained by X-ray diffraction, atomic force microscopy, scanning electron microscopy and Auger electron spectroscopy for thick (200-1100 nm) films grown on glass substrates. Transmission electron microscopy studies show that the 50-80 nm films contain a mixture of phases at all deposition temperatures. Transmission electron micrographs of annealed films and films deposited at high temperatures show a clear indication of grain growth.
H. P. Siriwardane et al., "Microstructure of Thin Iron Carbide Films Prepared in a Glow Discharge," Thin Solid Films, vol. 279, no. 1-2, pp. 155-161, Elsevier, Jun 1996.
The definitive version is available at https://doi.org/10.1016/0040-6090(95)08174-7
Materials Science and Engineering
Keywords and Phrases
Annealing; Atomic Force Microscopy; Auger Electron Spectroscopy; Glow Discharges; Grain Growth; High Temperature Effects; Iron Compounds; Microstructure; Scanning Electron Microscopy; Thick Films; Transmission Electron Microscopy; X ray Diffraction; Carbon Coated Copper Grids; Glass Substrates; Substrate Temperature; Thin Iron Carbide Films; Thin Films; Iron Carbide
International Standard Serial Number (ISSN)
Article - Journal
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