Gas Chromatographic-Inductively Coupled Plasma Emission Spectrometric Determination of Volatile Organometallic Species
Gas chromatography (GC) coupled with inductively coupled plasma emission spectrometry (ICPES) offers a powerful analytical tool for screening volatile organometallic compounds in complex mixtures, such as the products of coal conversion processes. Performance of a GC-ICPES system was evaluated for various organometallic compounds. Studies were also undertaken to explore the formation of volatile organoselenium compounds during gasification of coal spiked with inorganic selenium in the form of selenium sulfide. A number of organoselenium compounds were observed in the gasification by-products of the spiked coal.
D. O. Duebelbeis et al., "Gas Chromatographic-Inductively Coupled Plasma Emission Spectrometric Determination of Volatile Organometallic Species," Journal of Chromatography A, vol. 351, pp. 465-473, Elsevier, Jan 1986.
The definitive version is available at http://dx.doi.org/10.1016/S0021-9673(01)83523-8
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